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EQUIPMENT USED IN EXTRACTION PROSSESS
EQUIPMENT USED IN EXTRACTION PROSSESS. Principles and Equipment used in the following extraction processes:- Infusion, Decoction, Expression, Maceration, Percolation. Extraction involves the separation of medicinally active. Tissues from the inactive. Components by using selective solvents. In standard extraction procedures. Belladonna extract is obtained from the leaves of the plant Atropa belladonna. Source of drugs (active ingredients) may be plant or animal. Root, atropine from Belladonna leaves.
DISTILLATION
Raoult’s law and Henry’s law. Thoery of distillation of binary mixtures. Clasification and study of distillation equipment used for simple, vacuum, steam, reflux distillation, separation of azeotropes. What are the merits of boiling point diagram of a binary mixture? Write down the procedure of calculating equilibrium data of a binary mixture from its relative volatility value. (1999) [4 4]. Explain the method of azeotropic distillation in industrial scale. (1997) [6]. What is relative volatility? In a c...
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DRYING
Definition, purpose of drying, theory of drying, loss on drying, moisture content and equilibrium moisture content. Classification of dryers. Study of tray, rotary, vacuum, fluidized bed, freeze, spray and flash dryers. Classify dryers with examples. (2000) [3]. Describe the construction, operation and applications of Fluidized bed dryer. (2000) [10]. Mention the applications of freeze drying in pharmacy. (2000) [3]. Fluidized bed dryer(1999) [4]. What is the principle of freeze-drying? Falling rate peri...
EVAPORATION
Heat transfer to boiling liquid in evaporators. Physical and pharmaceutical factors affecting evaporation. Classification and study of pan, forced circulation, film, vacuum and multiple effect evaporator. Entrainment, prevention of foam and steam traps. Discuss the factors affecting evaporation. (2000) [6]. Classify evaporators with examples. (2000) [5]. With a neat sketch describe the working principle of a standard type vertical evaporator. (99) [10]. Discuss their application. (97) [4]. NB Thus no boi...