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All Chemist

Online community for chemists. Wednesday, 6 February 2013. Electronic Lab Notebooks- More organised, streamlined, secure and easier to search and share? For the past 6 years I worked as a research scientist in pharma industry working on synthesis of various molecules. All these years I documented the procedures in paper based notebooks and ended up having several sets of notebooks. Now today all of a sudden I started thinking why don’t we start using electronic lab notebooks. If anyone of you reading thi...

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Online community for chemists. Wednesday, 6 February 2013. Electronic Lab Notebooks- More organised, streamlined, secure and easier to search and share? For the past 6 years I worked as a research scientist in pharma industry working on synthesis of various molecules. All these years I documented the procedures in paper based notebooks and ended up having several sets of notebooks. Now today all of a sudden I started thinking why don’t we start using electronic lab notebooks. If anyone of you reading thi...

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All Chemist | allchemist.blogspot.com Reviews

https://allchemist.blogspot.com

Online community for chemists. Wednesday, 6 February 2013. Electronic Lab Notebooks- More organised, streamlined, secure and easier to search and share? For the past 6 years I worked as a research scientist in pharma industry working on synthesis of various molecules. All these years I documented the procedures in paper based notebooks and ended up having several sets of notebooks. Now today all of a sudden I started thinking why don’t we start using electronic lab notebooks. If anyone of you reading thi...

INTERNAL PAGES

allchemist.blogspot.com

1

All Chemist: Acyloin Condensation

http://allchemist.blogspot.com/2013/01/acyloin-condensation.html

Online community for chemists. Tuesday, 22 January 2013. Acyloin Condensation is a coupling reaction in which two carboxylic acid esters couple in the presence of metallic sodium under inert atmosphere to yield an α-hydroxyketone (also known as acyloin). If the condensation is carried out in the presence of proton donor like alcohol then reduction of ester to alcohol takes place. This reaction is also called as Bouveault-Blanc Reduction. Mechanism of Acyloin Condensation. The enediolate intermediate is t...

2

All Chemist: February 2012

http://allchemist.blogspot.com/2012_02_01_archive.html

Online community for chemists. Wednesday, 29 February 2012. Lithium diisopropylamide (LDA)-Preparation and usage. Lithium diisopropylamide is the chemical compound with the formula [(CH. LDA is cheaper than KDA and is more widely used. Organic Syntheses, Coll. Vol. 9, p.626 (1998); Vol. 72, p.62 (1995). NLi is a sufficiently strong base to deprotonate and cleave solvents such as Et. O, THF, and especially DME and HMP [(Me. PO] at temperatures above 0. NLi in these solvents. However, we have found tha...

3

All Chemist: September 2011

http://allchemist.blogspot.com/2011_09_01_archive.html

Online community for chemists. Thursday, 22 September 2011. Sulfuryl chloride is an inorganic compound with the formula SO. At room temperature, it is a colorless liquid with a pungent odor. Sulfuryl chloride is not found in nature, as can be inferred from its rapid hydrolysis. Sulfuryl chloride is commonly confused with thionyl chloride, SOCl. Sulfur is tetrahedral in SO. Is prepared by the reaction of sulfur dioxide and chlorine in the presence of a catalyst, such as activated carbon. Upon standing, SO.

4

All Chemist: April 2012

http://allchemist.blogspot.com/2012_04_01_archive.html

Online community for chemists. Wednesday, 25 April 2012. Below is the list of solvents along with density, melting point, boiling point, Formula weight. I have also inlcuded CAS no so that it will be helpful to you during your work. Please bring to my notice if there is any mistake in this list.:). Ethylene glycol dimethyl ether. Wednesday, April 25, 2012. Links to this post. Subscribe to: Posts (Atom). There was an error in this gadget. View my complete profile.

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All Chemist: December 2012

http://allchemist.blogspot.com/2012_12_01_archive.html

Online community for chemists. Sunday, 23 December 2012. Below mentioned are some of the techniques which I do. I just mentioned the rough idea and not a very detailed procedure here. Try to dissolve your compound in acetone. If it doesn't dissolve in acetone at rt then try to heat gently to make it dissolve. Then bring the solution to rt and try to add water slowly (your compound should be water insoluble) and see whether your compounds precipitates out pure or not. Dissolve your compound in minimum amo...

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allchemist.blogspot.com

All Chemist

Online community for chemists. Wednesday, 6 February 2013. Electronic Lab Notebooks- More organised, streamlined, secure and easier to search and share? For the past 6 years I worked as a research scientist in pharma industry working on synthesis of various molecules. All these years I documented the procedures in paper based notebooks and ended up having several sets of notebooks. Now today all of a sudden I started thinking why don’t we start using electronic lab notebooks. If anyone of you reading thi...

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