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Chemical Analysis: two applications of alkalimetry - The Scientific Amateur
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Diversions in chemistry, optics, electronics, and other hobbies. Chemical Analysis: two applications of alkalimetry. Jun 6th, 2008 at 7:37 AM. A Determination of Aspirin. So the usual practice goes. In truth it's not quite so simple. One difficulty, which I've never seen mentioned in undergraduate labs, is that the alcohol used to dissolve the tablet can be slightly acidic. Therefore a blank must be carried through, as I discuss in How to Titrate. Mass = 0.376 g): 29.10 mL 0.0617M NaOH used. A solution o...
How to Titrate - The Scientific Amateur
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Diversions in chemistry, optics, electronics, and other hobbies. May 18th, 2008 at 9:38 AM. Both in first- and second-year college lab classes in chemistry, here in the Seattle junior colleges anyway, require students to conduct at least one or two titrations, always using sodium hydroxide and phenolphthalein to determine a weak acid. Molecular weight determinations of organic acids are popular student labs. 1 Know your buret. The better burets have the graduations etched or engraved into the glass, whic...
June 2008 - The Scientific Amateur
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Diversions in chemistry, optics, electronics, and other hobbies. 09:02 pm: Chemical Analysis: alkalimetric adventures with sodium hydroxide. 07:37 am: Chemical Analysis: two applications of alkalimetry. 12:45 pm: Chemical Analysis: determining melting points with the Thiele-Dennis tube. 09:08 pm: Chemical Analysis: preparation of various acids for possible use as alkalimetric standards. 10:28 am: Organic Synthesis: the final failure of the sebacic acid preparation. View my Tags page.
Chemical Analysis: alkalimetric adventures with sodium hydroxide - The Scientific Amateur
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Diversions in chemistry, optics, electronics, and other hobbies. Chemical Analysis: alkalimetric adventures with sodium hydroxide. Jun 3rd, 2008 at 9:02 PM. And is usually carried out with better supplies than I have. The glassware is easy enough to get. I've already talked a little about burets and how to use them; $20 will get you a serviceable low-end model (e.g. this one. Aside from equipment, volumetric analysis requires certain chemicals of trustworthy purity, called primary standards. In most case...
Reheating: adventures with borax and potassium tetroxalate - The Scientific Amateur
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Diversions in chemistry, optics, electronics, and other hobbies. Reheating: adventures with borax and potassium tetroxalate. May 20th, 2008 at 8:39 AM. Be stable. Borax has a tendency to effloresce, lose water of crystallization, although it happens slowly in a well-closed container. Potassium tetroxalate, at least according to the Merck Index 11th edition, is stable to air. But these crystals, too, began to deliquesce on storage. Seeing this, I intensified the search for more information on potassiu...
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Left Conservative – Safe Spaces and Weird Rituals
Safe Spaces and Weird Rituals. Self-Segregation: Forming Communities or Destroying Them? Danah boyd on the ever interesting topic of the Big Sort. And yet, what Facebook does do is mirror and magnify a trend that’s been unfolding in the United States for the last twenty years, a trend of self-segregation that is enabled by technology in all sorts of complicated ways. January 11, 2017. January 11, 2017. Sometimes Rules Aren’t the Issue. December 29, 2016. When many lower-income Americans are feeling isola...
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The Scientific Amateur
Diversions in chemistry, optics, electronics, and other hobbies. Chemical Analysis: a successful gravimetric analysis of magnesium. Jun 20th, 2008 at 12:35 PM. Chemical Analysis: a failed gravimetric analysis of magnesium. Jun 19th, 2008 at 6:51 PM. Volumetric methods also suffer from a few disadvantages. Not all chemical species, for example, undergo reactions easily adaptable to titration—the alkali metals, for example, or aluminum. Other species do undergo characteristic reactions, but r...Gravimetric...
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