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The Neo Chemist | A Chemistry blog!

Cyclopentenone: Methylation with Methyl Lithium. December 20, 2016. I am doing following Methylation Reaction using Methyl Lithium in Diethyl Ether (1.6 M). Starting material was purified over flash silica and some fractions came with an upper spot that was not UV active. This starting material is UV active while the product is not as expected. 220 mg of the solid SM was used for the reaction. THF was […]. Raquo; Read more. May 4, 2015. Raquo; Read more. January 29, 2015. Raquo; Read more. April 20, 2014.

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The Neo Chemist | A Chemistry blog! | neochemist.com Reviews

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Cyclopentenone: Methylation with Methyl Lithium. December 20, 2016. I am doing following Methylation Reaction using Methyl Lithium in Diethyl Ether (1.6 M). Starting material was purified over flash silica and some fractions came with an upper spot that was not UV active. This starting material is UV active while the product is not as expected. 220 mg of the solid SM was used for the reaction. THF was […]. Raquo; Read more. May 4, 2015. Raquo; Read more. January 29, 2015. Raquo; Read more. April 20, 2014.

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The Neo Chemist | A Chemistry blog! | neochemist.com Reviews

https://neochemist.com

Cyclopentenone: Methylation with Methyl Lithium. December 20, 2016. I am doing following Methylation Reaction using Methyl Lithium in Diethyl Ether (1.6 M). Starting material was purified over flash silica and some fractions came with an upper spot that was not UV active. This starting material is UV active while the product is not as expected. 220 mg of the solid SM was used for the reaction. THF was […]. Raquo; Read more. May 4, 2015. Raquo; Read more. January 29, 2015. Raquo; Read more. April 20, 2014.

INTERNAL PAGES

neochemist.com

1

THF | Neochemist

https://www.neochemist.com/tag/thf

TBDMS or TBS Ether Deprotection with TBAF & AcOH. January 29, 2015. TBS or the TBDMS protection is a very versatile one for primary and secondary alcohols. Here we used it to selectively protect a cyclopentanol and then did some chemistry at the adjacent to get acetyl group there. Next, we need to remove this Silyl ether protection so that we can get the desired product in the reaction below. We tried […]. Raquo; Read more. Enter your email address:. TBDMS or TBS Ether Deprotection with TBAF & AcOH.

2

Hydrolysis Reaction Setup | Neochemist

https://www.neochemist.com/reaction/hydrolysis-reaction-setup

April 20, 2014. Here is a setup of reaction for hydrolysis of a methyl ester using Sodium hydroxide at 60 degree Celsius. The ester is methoxy methyl acrylate. We were required to get this acid after the hydrolysis so that we can convert it to acid chloride and finally to isocyanate. The isocyanate is then reacted with the amine counterpart to complete the synthesis of an Uridine Nucleoside analog. Leave a Reply Cancel reply. Your email address will not be published. Required fields are marked *.

3

AcOH | Neochemist

https://www.neochemist.com/tag/acoh

TBDMS or TBS Ether Deprotection with TBAF & AcOH. January 29, 2015. TBS or the TBDMS protection is a very versatile one for primary and secondary alcohols. Here we used it to selectively protect a cyclopentanol and then did some chemistry at the adjacent to get acetyl group there. Next, we need to remove this Silyl ether protection so that we can get the desired product in the reaction below. We tried […]. Raquo; Read more. Enter your email address:. TBDMS or TBS Ether Deprotection with TBAF & AcOH.

4

HCl | Neochemist

https://www.neochemist.com/tag/hcl

TBDMS or TBS Ether Deprotection with TBAF & AcOH. January 29, 2015. TBS or the TBDMS protection is a very versatile one for primary and secondary alcohols. Here we used it to selectively protect a cyclopentanol and then did some chemistry at the adjacent to get acetyl group there. Next, we need to remove this Silyl ether protection so that we can get the desired product in the reaction below. We tried […]. Raquo; Read more. Enter your email address:. TBDMS or TBS Ether Deprotection with TBAF & AcOH.

5

Mechanisms | Neochemist

https://www.neochemist.com/category/mechanisms

Conversion of Amine to Ketone. July 15, 2011. This is an important but less studied transformation of functional group in organic synthesis. This kind of reaction can go via imine formation which in turn is hydrolyzed to give ketone. Imine formation itself could be a two step process starting from N-halogenation followed by dehydrohalogenation using strong base. Imine can be hydrolyzed using strong acids such as Sulfuric Acid […]. Raquo; Read more. May 25, 2011. Raquo; Read more. March 2, 2011. February ...

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The Neo Chemist | A Chemistry blog!

Cyclopentenone: Methylation with Methyl Lithium. December 20, 2016. I am doing following Methylation Reaction using Methyl Lithium in Diethyl Ether (1.6 M). Starting material was purified over flash silica and some fractions came with an upper spot that was not UV active. This starting material is UV active while the product is not as expected. 220 mg of the solid SM was used for the reaction. THF was […]. Raquo; Read more. May 4, 2015. Raquo; Read more. January 29, 2015. Raquo; Read more. April 20, 2014.

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